Preparation and Properties of TaSi2-MoSi2 Borosilicate Glass Coating For SiCO Ceramic Heat Insulation Composite
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(Science and Technology on Advanced Ceramic Fibers and Composites Laboratory, National University of Defense Technology, Changsha 410073)

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TB35

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    Abstract:

    In order to improve the oxidation resistance and thermal shock resistance properties of the TaSi2-MoSi2 borosilicate glass coating for porous SiCO ceramic heat insulation composite, TaSi2-MoSi2 borosilicate glass coating on the surface of SiCO ceramic composites was prepared by brush-air sintering method. The microstructure and phase compositions of the coatings with the content of borosilicate glass respectively of 23%,31%,38%,41% were comparative observed by XRD and SEM with EDS. The thermal cycle experiment of the coated samples was performed by heating for 5 min at 1 500℃,then taking out to cool naturally down to room temperature.The result shows that the TaSi2-MoSi2 borosilicate glass coating with the content of borosilicate glass of 38% has fewest holes and cracks,the mass loss of the coating is -2.1%. It can be concluded that the TaSi2-MoSi2 glass coating with the content of borosilicate glass is 38% has the best oxidation resistance and thermal shock properties.

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History
  • Received:December 24,2015
  • Revised:
  • Adopted:
  • Online: January 11,2017
  • Published: