多孔Si3 N4 表面Al-Y-Si-O-N 陶瓷涂层的制备和表征
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西安交通大学金属材料强度国家重点实验室

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Fabrication and Characterization of Al-Y-Si-O-NCeramic Coating on Porous Si3 N4 Surface
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    摘要:

    采用溶胶-凝胶法,利用Al2O3 -Y2O3 -SiO2 溶胶中氧化物与基体中的Si3N4 颗粒反应制备一层致
    密Al-Y-Si-O-N 陶瓷涂层。主要研究了烧结温度对陶瓷涂层的组织和性能的影响,利用XRD 和EDS 分析涂
    层的相组成和微区元素组成,通过SEM 观察涂层的微观形貌。结果显示:在1 400益烧结时,能够制备出较为
    致密的陶瓷涂层,涂层由茁-sialon,Si2ON,SiO2 和非晶相组成;与基体相比,试样的吸水率下降了32. 8% ~
    90%,强度提高了2. 1% ~25. 9%。

    Abstract:

    Dense Al-Y-Si-O-N ceramic coating on the surface of porous Si3N4 was fabricated with oxides of
    Al2O3 -Y2O3 -SiO2 sol and Si3N4 of porous substrate using sol鄄gel method. Microstructure and properties of ceramic
    coating at the different temperatures were studied mainly. Phase composition and element component was analysed by
    XRD pattern and EDS,respectively, and microscopic morphology of surface and cross鄄section of coating was observed
    by the SEM. The ceramic coating is densified when the coating is sintered at 1 400益, and phase compositions of
    coating are consisted of 茁鄄sialon, Si2ON, SiO2 and amorphous phase. The results show that the water absorption of
    porous Si3N4 is decreased from 32. 8% to 90%, and the flexural strength of porous Si3N4 is increased from 2. 1% to
    25. 9%.

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王超.多孔Si3 N4 表面Al-Y-Si-O-N 陶瓷涂层的制备和表征[J].宇航材料工艺,2012,42(2).

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  • 在线发布日期: 2016-11-28
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