1Cr17Ni2螺栓氢脆断裂失效分析
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航天材料及工艺研究所,北京 100076

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TG115;TH131.3

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Hydrogen Embrittlement Fracture Failure Analysis of 1Cr17Ni2 Bolts
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Aerospace Research Institute of Materials & Processing Technology,Beijing 100076

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    摘要:

    某批次1Cr17Ni2螺栓在电机装配后放置期间发生断裂。通过宏/微观形貌分析、能谱分析等手段,确认其失效模式为脆性断裂,失效机理为氢脆。为探究失效原因并评估同规格其他批次螺栓的使用安全性,采用显微硬度、金相分析、氢含量测试对失效批次及其他两批次螺栓进行了比对试验,采用逐级加载法复现了螺栓失效模式。结果表明:失效批次螺栓内部氢含量显著高于其他批次,且其马氏体组织分布不均、晶粒粗大,导致局部氢富集,在装配应力作用下引发氢脆延迟断裂。在实验室环境下通过逐级加载法成功复现了失效批次失效现象,并评定其他两批次螺栓未呈现氢脆敏感性,可安全使用。逐级加载法可有效复现氢脆失效,可用于螺栓产品使用前的氢脆敏感性快速评定。

    Abstract:

    Fracture occurred in a batch of 1Cr17Ni2 bolts during storage after motor assembly.Through methods such as macro/microscopic morphology analysis and energy-dispersive spectroscopy(EDS),the failure mode was identified as brittle fracture with a mechanism of hydrogen embrittlement.To investigate the cause of failure and evaluate the use safety of bolts from other batches of the same specification,comparative tests including microhardness,metallographic analysis,and hydrogen content measurement were conducted on the failed batch and two other batches.The step-loading method was employed to reproduce the failure mode.The results indicate that the internal hydrogen content of the failed batch is significantly higher than that of the other batches.Furthermore,its in homogeneously distributed martensitic microstructure with coarse grains lead to local hydrogen enrichment,which triggered delayed hydrogen embrittlement fracture under assembly stress.In a laboratory environment,the failure phenomenon of the failed batch is successfully reproduced using the step-loading method.It is also evaluated that the other two batches show no hydrogen embrittlement susceptibility and are safe for use.This study demonstrates that the step-loading method can effectively reproduce hydrogen embrittlement failures and is suitable for the rapid assessment of hydrogen embrittlement susceptibility in bolt products prior to their use.

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王宇宁,王影,李西颜,卢克非,马兆庆.1Cr17Ni2螺栓氢脆断裂失效分析[J].宇航材料工艺,2026,56(2):109-116.

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  • 收稿日期:2025-12-02
  • 最后修改日期:2026-03-19
  • 录用日期:2026-01-26
  • 在线发布日期: 2026-05-07
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